*حسن شمران محمد لجين إبراهيم *قسم الكيمياء- وحدة البيئة- جامعة القادسية

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ISSN 1991-8690 1661 الترقيم الدولي - 0962 تقييم بعض المواصفات النوعية للخل المتداول في أسواق مدينة الديوانية *حسن شمران محمد لجين إبراهيم *قسم الكيمياء- وحدة البيئة- جامعة القادسية احمد جياد - كلية العلوم الخالصة (3.29-2.5) ph 15.6-3.5 1.50-0.13 1.11-0.06 110 (FAO and WHO2000, 8 4 0.51-0.26, 0.41-0.16, 0.51-0.25,0.31-0.01) FAO and WHO 2000 110

1988 A.pastenrianus 1975 1982 Nichol 1979, Cannin 1985 100 / Vinegar 8-4 Gerbi et al 1997 Bussy1975 500 2003 2003 4 ph ph-meter Buffer solution 30 Conner and 2003 1983 Allgeier 1976, De Ory et al 2002, Marshal et al 2000 50 400 10 Morales et al 2001 1988 0.2N 10 4 5 Bussy,1975 ; 1960 Shimadzu flame atomic 1987 absorption model, 6809 A.aceti De Ley et al 1989

1 (1) (ph) 3.29-2.5 0.31 0.3 2-0.01 3.4 - FAO and WHO 110 2.4 2000 WHO 0.51-0.25 FAO FAO and WHO,2000) %1.11 0.06 0.6% / 0.04% (1) 110 (WHO andfao 2000 1 5 0.98, 1.11 30 2 FAO and WHO and WHO,2000 ; 0.41-0.16 Myannmar2003) 5 0.51-0.26 FAO 8 1988 %10.9 1987 %15.6-3.5 %15.6 %13.4 1987 Bussy 1975 % - 4 1 3% %1.50-0.13 0.06%

الجدول رقم )1( بعض المحددات التي تبين خصائص الخل. الجدول رقم )2( تركيز بعض العناصر الثقيلة في عينات الخل المدروسة ( جزء بالمليون جزء( 1 -الجنددددي,محمدددد مم دددا )1983(. الغددد اء وال غ ددددة,دا الفكدددددر العربدددددش لللمدددددر,المجلد الةال,ال بعدددددة االولى,القاهرة ص 126-123. 2 -الددديلي باسدد كام,كامدد حمددودر الركددابش ) 1988 ). االغ دة و ا ة ال عليم العالش والبح العلمش,جامعة الموص,مددردة دا الك ب لل باعة واللمر جامعدة الموص ص 296-295. 3 -الرجب,وفداء حسين,حسدن محمدد علدش القد ا )1982). اساسدديال علددم االحيدداء المجاردددة الغدد ا ش,و ا ة ال علددديم العدددالش والبحددد العلمش,جامعدددة الموصددد,ال بعة االولى,م داب مددرددة دا الك دب لل باعدة واللمرجامعة الموص,ص 273-269. 4 -المواصدددددفة القياسدددددية قدددددم) 111 (/الخددددد /مجلددددد ال خ يط,الجاددددا المركدددد ر لل قيددددي والسددددي رة اللوعيدددددددددددددة,الجماو ددددددددددددددة العراقيدددددددددددددة )م ع 1897/111 (. 5 -ديلي,باس كام,صاد حسن الحكيم ) 1987 (. تحليد االغ دددددددددة, و ا ة ال علدددددددديم العددددددددالش والبحدددددددد العلمش,جامعة الموص,مددردة دا الك ب لل باعة واللمر جامعة الموص, ص 421-419.

Ley, Krieg NR, Holt JG. Bergey s manual of systematic bacteriaology. 1st ed Vol 1. Baltimore: Williams and Wilkins Co. p 267-279. ( ). 5-De Ory I, Romero LE, Cantero D; Journal of Food Engineering 52: 31-. (2002). 6-FAO and WHO Codex alimentarius Commission,Draft Revised Regionel Standard for Vinegar at30 June(CL2000/18-EURO).(2000). 7-Gerbi V, Zeppa G, Antonelli A, Natali N, Caracini A Mutivariate; Science Des Aliments 17:349-359.(1997). 8-Marshall J, Cotton M, Bal A Natural food antimicrobial systems: Chapter 24- acetic acid. 2nd ed. New York: Elsevier Applied Science Publishers. p 661. (2000). 9-Morales ML, Gustavo A, Gonzalez Jose A, Troncoso Ana M ; Journal of food technology 212: 676-682. (2001). 10-Myannmar Vinegar Dream World Co.,Ltd Myanmar (Burma) Myanmar Vinegar products specifications( Internet:htt://www.myanmar vinegar.com/).(2003). 11-Nickol GB Vinegar. In: Peppler HJ, Perlman D. Microbiology technology. 2 nd ed. New York: Academic Press. p 155-172. (1979). 9- صابر, محمد دوال )1999). نفحال علمية من القدرنن والسدلة, ال بعدة االولى,ملمدو ال مك بدة وشدلبير,ا بي, العرا. 3- صدمانو,شدمعون كدو كي (1988). السدي رة اللوعيدة والمواصفال القياسية لالغ دة, و ا ة ال عليم لعدالش والبحددددددد العلمش,جامعدددددددة الموصددددددد,ال بعدددددددة االولى,م داب مددرددة دا الك دب لل باعدة واللمدر جامعة الموص ص 144. 0- طهمددا, عبددد الحميددد محمددود ) 2003 (. خيددر االدام الخ, مكلون االعجا العلمدش, اال بعدون العلميدة, دا القلم, بيرول, لبلان. 6- عبددددددددد ال ددددددددي,محمددددددددود شاكر,فا دددددددد بلددددددددد عيسدددى ) 1989 (. الصدددلاعال الكيميا يدددة, و ا ة ال علدددديم العددددالش والبحدددد العلمش,هيئددددة المعاهددددد الفلية,دا اللقش لل باعة واللمر ص 230-228. 12- فدددود, دحيدددى حسدددن ) 1960 (. المراقبدددة الغ ا يدددة والمددنون الصددحية فددش ال صددلي الغدد ا ش,ال بعددة األولى, منسسة دا الك ب لل باعة واللمدر جامعدة الموص ص 186. 11 -م مددددد,عبددددد الباسددددط سدددديد, )2003 (. األعمددددا واللباتدال فدش ال دب اللبدور, الخد, مجلدة اللدواء االسالمش,قرنن وسلة. المصادر ايجنبية 1- Bussy T.H.De Vegetable food products luxuries,encyclopedia,ngmangroup d,london.p878-883.(1975). 2-Canning A; Journal of Food Sci Sept/ Oct: 20-21. (1985). 3-Conner HA, Allgeier RJ; Adv. Appl. Microbiol 20: 81-133. (1976). 4-De Ley J, Gollis M, Swings J Family VI In: Acetobacteriaceae Gillis, De 33

An evaluation of some quality standards for vinegar being sold in the local markets of Diwania province Abstract In this study we measured some qualifications which indicate the scope of contamination or idenfication of some kinds of vinegar existing in Diwania markets to qualitative Iraqi and international standards. Acidic factor (ph) has been checked between 2.5-3.29 for various samples, Total acidity has been checked by guidance of acetic acid ranging between 3.5-15.6 % for various samples of vinegar. The total ash is ranging between 0.06 1.11%. The total ratio of solid materials is ranging between 0.13-1.50 %. The results indicated that all these variables ranged within admissible limits for natural vinegar except the ratio of acetic acid in some samples examined which were higher than accepted limits (4-8 %). Some samples of vinegar under study have been examined to know the extent of their contamination due to some materials like Lead, Copper, iron and zinc. The results indicated that these samples contained one part from million parts as follows :- (0.01 0.31, 0.25 0.51, 0.16 0.41, 0.26 0.51), These ratios are with admissible limits according to Iraqi and international standards. 39